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https://hdl.handle.net/10442/19514
Εξειδίκευση τύπου : | Άρθρο σε επιστημονικό περιοδικό |
Τίτλος: | Eco-Friendly Recovery of Homogalacturonan-Rich Pectin from Flaxseed Cake via NADES Extraction |
Δημιουργός/Συγγραφέας: | Mazurek-Hołys, Aleksandra Górska, Ewa Tsirigotis-Maniecka, Marta [EL] Ζουμπανιώτη, Μαρία[EN] Zoumpanioti, Maria Bleha, Roman Pawlaczyk-Graja, Izabela |
Ημερομηνία: | 2025-09-19 |
Γλώσσα: | Αγγλικά |
ISSN: | 2073-4360 |
DOI: | 10.3390/polym17182532 |
Άλλο: | 41012295 |
Περίληψη: | Flaxseed polysaccharides (FLP) are bioactive macromolecules with valuable functional properties and applications in the food, pharmaceutical, and packaging industries. This study focused on obtaining high-purity pectin from flaxseed cake using sustainable extraction with natural deep eutectic solvents (NADES) based on choline chloride (ChCl) and citric acid (CA) The ChCl/CA system (1:1) resulted in the LU3 extract, which provided the best outcome, yielding the highest pectin recovery (36.88 mg/g), elevated uronic acid content (30.33% of sample; 68.15% of saccharides), and the lowest protein contamination (11.46%), confirming superior pectin purity. Structural (UV-Vis, FT-IR, GC-MS, GPC, LH-20) identified homogalacturonan with xylogalacturonan domains (53% DM) and a molecular weight range of 14-500 × 103 g/mol. Morphological and physicochemical characterization, including SEM/EDS imaging, zeta potential analysis, and rheological measurements, revealed that LU3 is an anionic, heterogeneous biopolymer exhibiting pH-dependent charge behavior. These properties underscore its potential as a safe and effective material for bio-industrial applications. Overall, the study demonstrates that NADES provide an eco-friendly and efficient medium for extracting high-quality pectin from flaxseed cake, offering a sustainable strategy for the valorization of flaxseed polysaccharides in bio-based products. |
Τίτλος πηγής δημοσίευσης: | Polymers |
Τόμος/Κεφάλαιο: | 17 |
Τεύχος: | 18 |
Θεματική Κατηγορία: | [EL] Βιοτεχνολογία[EN] Biotechnology [EL] Αναλυτική χημεία[EN] Analytical chemistry [EL] Χημική τεχνολογία[EN] Chemical technolgy [EL] Φασματοσκοπία[EN] Spectroscopy |
Λέξεις-Κλειδιά: | flaxseed cake homogalacturonan natural deep eutectic solvents pectin |
Χρηματοδότης: | Ministry of Science and Higher Education, Poland |
Κάτοχος πνευματικών δικαιωμάτων: | © 2025 by the authors. Licensee MDPI, Basel, Switzerland. |
Όροι και προϋποθέσεις δικαιωμάτων: | This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/ licenses/by/4.0/) |
Ηλεκτρονική διεύθυνση στον εκδότη (link): | https://doi.org/10.3390/polym17182532 |
Εμφανίζεται στις συλλογές: | Ινστιτούτο Χημικής Βιολογίας - Επιστημονικό έργο
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